No, however to answer my own question, in case anyone else has this situation:
The original volume set was set as LUN #00 and the new volume set was LUN #01. By removing the first raid set (thus the original volume set), Windows is unable to see LUN#00, therefore will not recognize LUN#01...
I recently added four 2TB drives and created a new raid set (#1)/volume, then copied the data from the original volume (raid set #0 - containing 750GB drives). After the copy, I shutdown the system, removed the drives from the cage and booted.
After booting, Win Server 2003 does not...